Study of an SmBO₃-ScBO₃system and new SmSc(BO₃)₂orthoborate

Kuznetsov A.B. Kokh K.A. Kononova N.G. Shevchenko V.S. Rashchenko S.V. Lapin I.N. Svetlichnyi V.A. Uralbekov B. Bolatov A. Simonova E.A. Kokh A.E.
14 February 2021 Royal Society of Chemistry

CrystEngComm
2021 #23 Issue 6 1482 - 1488 pp.

A new SmSc(BO₃)₂compound was discovered from the study of SmBO₃-ScBO₃by solid-state synthesis. The obtained compound was grown from a stoichiometric melt by a spontaneous crystallization method, and crystallizes in the space groupR3̄ with the cell parameters ofa= 4.8951(6) Å andc= 16.3012(2) Å. In addition, phase equilibria in this system in the 900-1300 °C temperature range were studied by X-ray diffraction and thermal analyses, as well as special diffusion experiments.

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Sobolev Institute of Geology and Mineralogy SB RAS, Novosibirsk, 630090, Russian Federation
Novosibirsk State University, Novosibirsk, 630090, Russian Federation
Tomsk State University, Tomsk, 634050, Russian Federation
Al-Farabi Kazakh National University, Almaty, 050040, Kazakhstan
Kemerovo State University, Kemerovo, 650000, Russian Federation

Sobolev Institute of Geology and Mineralogy SB RAS
Novosibirsk State University
Tomsk State University
Al-Farabi Kazakh National University
Kemerovo State University

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