Synthesis of New Symmetrical Diamidophosphates Based on meta-Phenylenediamine under Microwave Irradiation
Kuandykova A.B. Dzhiembaev B.Z. Burilov A.R. Akylbekov N.I. Chugunova E.A. Dobrynin A.B. Abyzbekova G.M.
June 2023Pleiades Publishing
Russian Journal of General Chemistry
2023#93Issue 61386 - 1390 pp.
Abstract: A new series of diphosphorylated amidophosphates was obtained as a result of the reaction of meta-phenylenediamine with dialkyl phosphites in the presence of CCl4 and triethylamine (Atherton–Todd reaction) under microwave irradiation. Structure of all the obtained amidophosphates was established on the basis of 31P, 1H, 13C NMR, IR spectroscopy and mass spectrometry methods, as well as single crystal X-ray diffraction and elemental analysis data.
Atherton–Todd reaction , dialkyl phosphites , meta-phenylenediamine , microwave irradiation
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Kazakh National Women‘s Teacher Training University, Almaty, 050000, Kazakhstan
A.E. Arbuzov Institute of Organic and Physical Chemistry, Federal Research Center “Kazan Scientific Center of the Russian Academy of Sciences”, Kazan, 420088, Russian Federation
Korkyt Ata Kyzylorda University, Kyzylorda, 120014, Kazakhstan
Kazakh National Women‘s Teacher Training University
A.E. Arbuzov Institute of Organic and Physical Chemistry
Korkyt Ata Kyzylorda University
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