Evaluation of the Influence of Grain Sizes of Nanostructured WO3 Ceramics on the Resistance to Radiation-Induced Softening


Kadyrzhanov D.B. Kozlovskiy A.L. Zdorovets M.V. Kenzhina I.E. Shlimas D.I.
February 2023MDPI

Materials
2023#16Issue 3

The main purpose of this study is to test a hypothesis about the effect of grain size on the resistance to destruction and changes in the strength and mechanical properties of oxide ceramics subjected to irradiation. WO3 powders were chosen as objects of study, which have a number of unique properties that meet the requirements for their use as a basis for inert matrices of dispersed nuclear fuel. The grain-size variation in WO3 ceramics was investigated by mechanochemical grinding of powders with different grinding speeds. Grinding conditions were experimentally selected to obtain powders with a high degree of size homogeneity, which were used for further research. During evaluation of the strength properties, it was found that a decrease in the grain size leads to an increase in the crack resistance, as well as the hardness of ceramics. The increase in strength properties can be explained by an increase in the dislocation density and the volume contribution of grain boundaries, which lead to hardening and an increase in resistance. During determination of the radiation damage resistance, it was found that a decrease in grain size to 50–70 nm leads to a decrease in the degree of radiation damage and the preservation of the resistance of irradiated ceramics to destruction and cracking.

hardening , hardness , nanosized grains , radiation damage , strength , WO3 ceramics

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Engineering Profile Laboratory, L.N. Gumilyov Eurasian National University, Nur-Sultan, 010008, Kazakhstan
Department of General Physics, Satbayev University, Almaty, 050032, Kazakhstan
Department of Intelligent Information Technologies, Ural Federal University, Yekaterinburg, 620075, Russian Federation
Advanced Electronics Development Laboratory, Kazakh-British Technical University, 59 Tole bi St., Almaty, 050000, Kazakhstan

Engineering Profile Laboratory
Department of General Physics
Department of Intelligent Information Technologies
Advanced Electronics Development Laboratory

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